Practical’s in Pharmaceutical Organic Chemistry - II

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Publisher: Prime Publishing House
ISBN: 9789395596978
Year: 2024
Pages: 114

This practical book on Pharmaceutical Organic Chemistry is designed to provide a clear and simplified understanding of essential laboratory techniques and experimental concepts in organic chemistry. It serves as a comprehensive guide for students to develop practical skills through well-structured experiments, making complex procedures easy to perform and understand.

The book includes detailed theoretical backgrounds for each experiment, explaining the underlying principles to strengthen conceptual clarity. It covers a wide range of practical topics such as recrystallization, steam distillation, qualitative analysis, separation and identification of organic compounds, determination of physical constants, and synthesis of important organic compounds. Each procedure is presented in a step-by-step manner and supported with appropriate diagrams to enhance learning and accuracy in laboratory work.

With its systematic approach and easy-to-follow language, this book helps students build confidence in performing experiments and understanding their significance. It is a valuable resource for strengthening practical knowledge, improving analytical skills, and achieving better performance in laboratory examinations and professional practice.

I. Limit Test of the following
A. Introduction of Pharmaceutical Organic Chemistry
B. Laboratory Safety in Pharmaceutical Organic Chemistry
C. Common Laboratory Equipment, Apparatus, Glass Wares
D. Experiments Involving Laboratory Techniques
Experiment 1 : To Perform Recrystallization of Given Compound
Experiment 2 : To Perform Steam Distillation for Separation of Given Mixture.
E. Introduction to Separation and Systematic identification of
Binary Mixture of Organic Compounds by Qualitative Analysis.
1. Solubility Test
2. Detection of Elements (Halogens, Nitrogen and Sulphur) in
An Organic Compound
3. Systematically identify the functional groups in the given organic compound and
perform the confirmatory tests after identifying the functional groups
4. Determination of Physical Constant (Melting/Boiling Point)
5. The Preparation of Derivatives of Organic Compounds
F. Qualitative Organic Analysis
Experiment 3 : To Perform Separation and Qualitative Analysis
of Given Organic Mixture
G. Determination of Saponification Value of Oil Sample
Experiment 4 : To determine the Saponification Value of the
Given Sample of Oil
H. Synthesis of Organic Compounds
Experiment 5 : To Synthesize Acetanilide from Aniline
Experiment 6 : To Synthesize Phenyl benzoate from Benzoyl Chloride
Experiment 7 : To Synthesize 2,4,6-Tribromoaniline from Aniline
Experiment 8 : To Synthesize m-Dinitrobenzene (1,3-Dinitrobenzene)
from Nitrobenzene
Experiment 9 : To Synthesize Benzanilide from Aniline
Experiment 10 : To Synthesize p-Bromo acetanilide from Acetanilide
Experiment 11 : To Synthesize Dibenzal acetone from Benzaldehyde
Experiment 12 : To Synthesize Acetyl salicylic acid (Aspirin)
from Salicylic acid
Experiment 13 : To Synthesize Phthalimide from Phthalic Anhydride
Experiment 14 : To Synthesize Benzil from Benzoin
I. Common Laboratory Reagents

A book as per the latest syllabus given by Pharmacy Council of India (PCI) New Delhi for B.Pharm students of all Indian Universities

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